Visible light photocatalytic oxidation of NO using g-C3N4 nanosheets: stability, kinetics, and effect of humidity

Sofia Stefa, Evangelia Skliri, Emmanouil Gagaoudakis, George Kiriakidis, Dimitrios Kotzias, Panos Papagiannakopoulos, M. Konsolakis, Samuel Mao, Vassilios Binas

    Research output: Contribution to journalArticlepeer-review

    2 Scopus citations

    Abstract

    Heterogeneous photocatalysis is a promising technology for the degradation of environmental pollutants. In this work, g-C3N4 nanosheets were employed as a visible light photocatalyst to investigate the stability, kinetics and to understand the impact of humidity on the photocatalytic oxidation of nitric oxide (NO). Graphitic carbon nitride (g-C3N4) with unique physicochemical properties proves to be a promising photocatalytic material. Visible light active g-C3N4 nanosheets were successfully synthesized by thermal polycondensation of melamine followed by thermal exfoliation. Compared with the bulk carbon nitride, g-C3N4 nanosheets show significant NO removal efficiency (68%), followed by excellent stability after 5 cycles of photocatalytic oxidation under visible LED light illumination. Furthermore, photocatalytic oxidation of NO at various humidity levels revealed the significant role of humidity in photocatalytic NO removal. Finally, the initial uptake coefficients γ0,geo, and γ0,BET of NO on g-C3N4 nanosheets were determined to be 1.0 × 10− 5 and 1.58 × 10− 9, respectively, and were found to decrease with increasing humidity. It appears that the photocatalytic removal of NO happens primarily on the surface of the g-C3N4 nanosheet.

    Original languageBritish English
    Article number451
    JournalApplied Physics A: Materials Science and Processing
    Volume130
    Issue number6
    DOIs
    StatePublished - Jun 2024

    Keywords

    • g-CN nanosheets
    • Kinetic analysis
    • LED visible-light photocatalysis
    • NO removal
    • Stability

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