TY - JOUR
T1 - Process optimization for the preparation of activated carbon from Jatropha hull using response surface methodology
AU - Duan, X.
AU - Peng, Jinhui
AU - Srinivasakannan, C.
AU - Zhang, L.
AU - Xia, H.
AU - Yang, K.
AU - Zhang, Z.
N1 - Funding Information:
The authors would like to express their gratitude to the National Key Technology R&D Program of China (No. 2007BAD32B04) for financial support.
PY - 2011
Y1 - 2011
N2 - Preparation of activated carbon has been attempted using CO2 as the activating agent from Jatropha hull, one of the popular feed stocks for biodiesel manufacture. The response surface methodology technique is utilized to optimize the process conditions. The influences of the three major parameters, activation temperature, activation time, and CO2 flow rate on the properties of activated carbon, are investigated using analysis of variance to identify the significant parameters. The optimum conditions for preparation of activated carbon has been identified to be an activation temperature of 950°C, activation time of 40 min, and CO2 flow rate of 500 ml/min, an iodine number of 1,008 mg/g, and a yield of 18% were obtained, respectively. The BET surface area evaluated using nitrogen adsorption isotherm for the optimal sample corresponds to a 1,207 m2/g, with the pore volume of 0.86 cc/g. The activated carbon is heteroporous with the micropore volume contributing to 58%.
AB - Preparation of activated carbon has been attempted using CO2 as the activating agent from Jatropha hull, one of the popular feed stocks for biodiesel manufacture. The response surface methodology technique is utilized to optimize the process conditions. The influences of the three major parameters, activation temperature, activation time, and CO2 flow rate on the properties of activated carbon, are investigated using analysis of variance to identify the significant parameters. The optimum conditions for preparation of activated carbon has been identified to be an activation temperature of 950°C, activation time of 40 min, and CO2 flow rate of 500 ml/min, an iodine number of 1,008 mg/g, and a yield of 18% were obtained, respectively. The BET surface area evaluated using nitrogen adsorption isotherm for the optimal sample corresponds to a 1,207 m2/g, with the pore volume of 0.86 cc/g. The activated carbon is heteroporous with the micropore volume contributing to 58%.
KW - Activated carbon
KW - Biomass
KW - Iodine adsorption
KW - Optimization
KW - Response surface methodology
KW - Yield
UR - http://www.scopus.com/inward/record.url?scp=79961126027&partnerID=8YFLogxK
U2 - 10.1080/15567030903515047
DO - 10.1080/15567030903515047
M3 - Article
AN - SCOPUS:79961126027
SN - 1556-7036
VL - 33
SP - 2005
EP - 2017
JO - Energy Sources, Part A: Recovery, Utilization and Environmental Effects
JF - Energy Sources, Part A: Recovery, Utilization and Environmental Effects
IS - 21
ER -
