TY - JOUR
T1 - Mesoporous cubic Ia3d materials for the preparation of fine chemicals
T2 - Synthesis of jasminaldehyde
AU - Prabhu, Azhagapillai
AU - Palanichamy, Muthaiahpillai
PY - 2013/3/1
Y1 - 2013/3/1
N2 - The synthesis of mesoporous Al-KIT-6 is synthesized by direct hydrothermal method with different Si/Al ratios (20, 30, 50, 100 and 150) were characterized by XRD, ICP-AES, BET, SEM and HR-TEM. Mesoporous Al-KIT-6 was synthesized from assembly of polymer surfactant micelle as a template in acidic media. Mesoporous Al-KIT-6 was good phase purity from XRD analysis. The HR-TEM picture of Al-KIT-6 (50) showed formation of particles of cubic morphology and SEM images are also shown rod like morphology. α-n-Amylcinnamaldehyde (jasminaldehyde) has been prepared with high selectivity and using low ratios of benzaldehyde/heptanal by means of mesoporous Al-KIT-6 molecular sieves.
AB - The synthesis of mesoporous Al-KIT-6 is synthesized by direct hydrothermal method with different Si/Al ratios (20, 30, 50, 100 and 150) were characterized by XRD, ICP-AES, BET, SEM and HR-TEM. Mesoporous Al-KIT-6 was synthesized from assembly of polymer surfactant micelle as a template in acidic media. Mesoporous Al-KIT-6 was good phase purity from XRD analysis. The HR-TEM picture of Al-KIT-6 (50) showed formation of particles of cubic morphology and SEM images are also shown rod like morphology. α-n-Amylcinnamaldehyde (jasminaldehyde) has been prepared with high selectivity and using low ratios of benzaldehyde/heptanal by means of mesoporous Al-KIT-6 molecular sieves.
KW - 1-Heptanal
KW - Al-KIT-6
KW - Benzaldehyde
KW - Jasminaldehyde
KW - Mesoporous cubic ia3d
UR - http://www.scopus.com/inward/record.url?scp=84868229977&partnerID=8YFLogxK
U2 - 10.1016/j.micromeso.2012.09.020
DO - 10.1016/j.micromeso.2012.09.020
M3 - Article
AN - SCOPUS:84868229977
SN - 1387-1811
VL - 168
SP - 126
EP - 131
JO - Microporous and Mesoporous Materials
JF - Microporous and Mesoporous Materials
ER -