Mesoporous cubic Ia3d materials for the preparation of fine chemicals: Synthesis of jasminaldehyde

Azhagapillai Prabhu, Muthaiahpillai Palanichamy

    Research output: Contribution to journalArticlepeer-review

    15 Scopus citations

    Abstract

    The synthesis of mesoporous Al-KIT-6 is synthesized by direct hydrothermal method with different Si/Al ratios (20, 30, 50, 100 and 150) were characterized by XRD, ICP-AES, BET, SEM and HR-TEM. Mesoporous Al-KIT-6 was synthesized from assembly of polymer surfactant micelle as a template in acidic media. Mesoporous Al-KIT-6 was good phase purity from XRD analysis. The HR-TEM picture of Al-KIT-6 (50) showed formation of particles of cubic morphology and SEM images are also shown rod like morphology. α-n-Amylcinnamaldehyde (jasminaldehyde) has been prepared with high selectivity and using low ratios of benzaldehyde/heptanal by means of mesoporous Al-KIT-6 molecular sieves.

    Original languageBritish English
    Pages (from-to)126-131
    Number of pages6
    JournalMicroporous and Mesoporous Materials
    Volume168
    DOIs
    StatePublished - 1 Mar 2013

    Keywords

    • 1-Heptanal
    • Al-KIT-6
    • Benzaldehyde
    • Jasminaldehyde
    • Mesoporous cubic ia3d

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