7-Fluoro-isatin-1,4-dioxane (1/1)

Kenneth Shankland; Charlotte K. Leech; Sharmarke Mohamed; Sarah A. Barnett; Derek A. Tocher

doi:10.1107/S1600536807035258

7-Fluoro-isatin-1,4-dioxane (1/1)

Kenneth Shankland, Charlotte K. Leech, Sharmarke Mohamed, Sarah A. Barnett, Derek A. Tocher

Chemistry

Research output: Contribution to journal › Article › peer-review

12 Scopus citations

Abstract

The title 1,4-dioxane solvate, C8H4FNO2·C4H8O2, was isolated during a manual crystallization screen on 7-fluoro-isatin (7-fluoro-indoline-2,3-dione) . The 7-fluoro-isatin mol-ecule occupies a general position and each of the independent mol-ecules of 1,4-dioxane is disposed about a centre of inversion, with half of each in the asymmetric unit. Hydrogen-bonded ribbons of 7-fluoro-isatin are linked by 1,4-dioxane to form sheets parallel to (30 ). Whilst one solvent mol-ecule has an active role in the sheet formation, the other simply fills the cavity formed within the sheet.

Original language	British English
Pages (from-to)	o3574
Journal	Acta Crystallographica Section E: Structure Reports Online
Volume	63
Issue number	8
DOIs	https://doi.org/10.1107/S1600536807035258
State	Published - 31 Jul 2007

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title = "7-Fluoro-isatin-1,4-dioxane (1/1)",

abstract = "The title 1,4-dioxane solvate, C8H4FNO2·C4H8O2, was isolated during a manual crystallization screen on 7-fluoro-isatin (7-fluoro-indoline-2,3-dione) . The 7-fluoro-isatin mol-ecule occupies a general position and each of the independent mol-ecules of 1,4-dioxane is disposed about a centre of inversion, with half of each in the asymmetric unit. Hydrogen-bonded ribbons of 7-fluoro-isatin are linked by 1,4-dioxane to form sheets parallel to (30 ). Whilst one solvent mol-ecule has an active role in the sheet formation, the other simply fills the cavity formed within the sheet.",

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T1 - 7-Fluoro-isatin-1,4-dioxane (1/1)

AU - Shankland, Kenneth

AU - Leech, Charlotte K.

AU - Mohamed, Sharmarke

AU - Barnett, Sarah A.

AU - Tocher, Derek A.

PY - 2007/7/31

Y1 - 2007/7/31

N2 - The title 1,4-dioxane solvate, C8H4FNO2·C4H8O2, was isolated during a manual crystallization screen on 7-fluoro-isatin (7-fluoro-indoline-2,3-dione) . The 7-fluoro-isatin mol-ecule occupies a general position and each of the independent mol-ecules of 1,4-dioxane is disposed about a centre of inversion, with half of each in the asymmetric unit. Hydrogen-bonded ribbons of 7-fluoro-isatin are linked by 1,4-dioxane to form sheets parallel to (30 ). Whilst one solvent mol-ecule has an active role in the sheet formation, the other simply fills the cavity formed within the sheet.

AB - The title 1,4-dioxane solvate, C8H4FNO2·C4H8O2, was isolated during a manual crystallization screen on 7-fluoro-isatin (7-fluoro-indoline-2,3-dione) . The 7-fluoro-isatin mol-ecule occupies a general position and each of the independent mol-ecules of 1,4-dioxane is disposed about a centre of inversion, with half of each in the asymmetric unit. Hydrogen-bonded ribbons of 7-fluoro-isatin are linked by 1,4-dioxane to form sheets parallel to (30 ). Whilst one solvent mol-ecule has an active role in the sheet formation, the other simply fills the cavity formed within the sheet.

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7-Fluoro-isatin-1,4-dioxane (1/1)

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